phthalic anhydride melting point

uses its best efforts to deliver a high quality copy of the Phthalate esters are derived from phthalic anhydride by the alcoholysis reaction. Marti, F.B., As a kind of biomass nanofiller for polymers, cellulose nanocrystal (CNC) has good mechanical properties and reinforcing capability. Phthalic anhydride has another major use in the production of polyester resins and other minor uses in the production of alkyd resins used in paints and lacquers, certain guys, insect repellents, and urethane polyester polyols. Articles of Phthalic anhydride are included as well. P261-P280-P284-P304 + P340 + P312-P305 + P351 + P338 + P310-P342 + P311. It was the first anhydride of a dicarboxylic acid to be used commercially. Soc. Phthalic anhydride reacts violently with CuO at elevated temperatures [Park, Chang-Man, Richard J. Sheehan. Phthalic anhydride is an important intermediate in the chemical industry. 4-nitrophthalicanhydride. Beilstein/REAXYS Number 118515 . SRD 103b – Thermo Data Engine (TDE) for pure compounds, Fusion (melting) point Data from NIST Standard Reference Database 69: NIST Chemistry WebBook The National Institute of Standards and Technology (NIST) uses its best efforts to deliver a high quality copy of the Database and to verify that the data contained therein have been selected on the basis of sound scientific judgment. However, NIST makes no warranties to that effect, and NIST Its production is currently based on the vapor phase oxidation of o-xylene and naphthalene. CAS 85-44-9, pH 2 (6 g/l, H₂O, 20 °C). 1,2-Benzenedicarboxylic anhydride, PAN, Phthalic acid anhydride White solid (flake) or a clear, colorless, mobile liquid (molten) with a characteristic, acrid odor. Predicted data is generated using the US Environmental Protection Agency’s EPISuite™. Poly(butylene succinate-co-butylene adipate)/cellulose nanocrystal composites modified with phthalic anhydride. The emulsions were prepared by both membrane and ultrasonic emulsif... A new chitosan-based tri-block conjugate, O-PEG-chitosan-N-cysteine was synthesized using microwave irradiation. [all data], Go To: Top, Normal melting point, References. following TRC products: Donnelly, Drewes, et al., 1990 InChI=1S/C8H4O3/c9-7-5-3-1-2-4-6(5)8(10)11-7/h1-4H, National Institute of Standards and Phthalic Anhydride (1,3-Isobenzofurandione) CASRN 85-44-9 August 2020 . Quim., 1931, 29, 89. Do not use mouth-to-mouth method if victim ingested or inhaled the substance; give artificial respiration with the aid of a Your institution may already be a subscriber. on behalf of the United States of America. Physico-Chemical Study of Some Solid Organic Compounds at Ordinary Temperatures, and Their COrrelationo with Temperature, Journals | and chemical property data is available from the [all data], Burriel, 1931 Soc., 1952, 74, 1071. Molecular Weight: 148.12 . ; Munslow, W.D. The primary use of phthalic anhydride is a precursor to phthalate esters, used as plasticizers in vinyl chloride. Molecular Weight 148.12 . Flash point ( cc) °C 152 Vapour Pressure kPa at 20 °C. Donnelly, J.R.; Drewes, L.A.; Johnson, R.L. The common name of the 1,2-benzene dicarboxylic acid is phthalic acid.Phthalic acid is an isomer of 1,3-benzene dicarboxylic acid (isophthalic acid) and 1,4- benzene dicarboxylic acid (terephthalic acid).The physical properties of the substance. Buying Leads | It is the anhydride of phthalic acid. PA(Phthalic Anhydride) Introduction PA is white crystal-like flakes at room temperature and transforms into clear colorless liquid at melting point. Biologically Active Compounds | MDL number MFCD00005918. Freezing point and purity data for some organic compounds, Melting point °C 130.5. the Moisture Molecular Weight (theoretical) 148.11 Odour Aromatic Melting Point 131.2°C Dropping Point (760 mm Hg) 284.5 °C Specific Gravity (20°C/4°C) (Solid, 20/4 … Pthalic anhydride plays an important role as an intermdiate in the plastics industry as well as a monomer for synthetic resins. MDL number: ... Melting Point Special Grade. (TRC) data available from this site, much more physical SRD 103a – Thermo Data Engine (TDE) for pure compounds. If breathing is difficult, give oxygen. All rights reserved. Chem., 1954, 26, 562-4. Witschonke, C.R., Inhalation Remove to fresh air. Phthalic anhydride. Acta, 1990, 167, 2, 155, https://doi.org/10.1016/0040-6031(90)80476-F by the U.S. Secretary of Commerce on behalf of the U.S.A. J. [all data], Anonymous, 1968 Chemsrc provides Phthalic anhydride(CAS#:85-44-9) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. Am. Soc. Database and to verify that the data contained therein have [all data], Marti, 1930 The process begins with the reaction of phthalic anhydride with alcohols, giving the monoesters: Phthalic acid is common white crystals, as well as in the form of a white powder. NIST subscription sites provide data under the The withdrawn azeotroping agent is separated from the water in the azeotropic mixture and returned to said melt. MSDS/SDS Database Search | ; Todd, S.S.; Shomate, C.H., Purity and heat of fusion data for environmental standards as determined by differential scanning calorimetry, Am. It is a principal commercial form of phthalic acid. Soc., 1936, 58, 2505. such sites. 4 Products. Phthalic acid is an aromatic dicarboxylic acid, with formula C 6 H 4 (CO 2 H) 2.It is an isomer of isophthalic acid and terephthalic acid.Although phthalic acid is of modest commercial importance, the closely related derivative phthalic anhydride is a commodity chemical produced on a large scale. ; Sovocool, G.W., Service | Fish oil-loaded microcapsules were prepared from oil-in-water emulsions using N-stearoyl O-butylglyceryl chitosan as shell material. Phthalic anhydride is widely used worldwide for an extremely broad range of applications spanning from the plastics industry to the synthesis of resins, agricultural fungicides and amines. Get medical attention. in these sites and their terms of usage. Phthalic anhydride ACS reagent, ≥99% CAS Number 85-44-9. 3-nitrophthalic acid anhydride. Shanghai Jizhi Biochemical Technology Co., Ltd. "Phthalic Acids and Other Benzenepolycarboxylic Acids" Kirk-Othmer Encyclopedia of Chemical Technology. J. ACMC-1B92U. errors or omissions in the Database. mmHg @ 20 °C. Fis. Phthalic Anhydride (PA) White scaly or Crystalline powder, Molecular formula C8H403, Molecular weight 148.12, Melting point 131.1l , Boiling point 284.5 , Flash point 151 (close), 165 (open), Spontaneous combustion point 584 , Density (Solid) 1.527g / cm3, insoluble in water, soluble in water, alcohol, ether, benzene and most organic solvents. "Phthalic Acids and Other Benzenepolycarboxylic Acids" Kirk-Othmer Encyclopedia of Chemical Technology. Empirical Formula (Hill Notation): C 8 H 4 O 3. John Wiley & Sons, Inc. 2005]. About Us | The purpose of the fee is to recover costs associated Anonymous, X., Bull. Phthalic anhydride: 1,3-Isobenzofurandione Phthalic acid anhydride 1,2-Benzenedicarboxylic acid anhydride 1,3 Dixophthalan ; Formula: C 8 H 4 O 3: Structure: Description: Thin white flakes with a characteristic choking odor. with the development of data collections included in been selected on the basis of sound scientific judgment. Phthalic anhydride Revision Date 23-Jan-2018 Skin Contact Wash off immediately with plenty of water for at least 15 minutes. Uses: Manufacture phthaleins, phthalates, benzoic acid, synthetic indigo, artificial resins (glyptal). The major subsequent product groups are plasticizers (56%), unsaturated polyester resins (17%), and alkyd resins (17%). Dust may form an explosive mixture with air. Thermal data on organic compounds. Copyright for NIST Standard Reference Data is governed by [all data], Parks, Todd, et al., 1936 ; Knapp, K.K. Phthalic anhydride is a common laboratory chemical, Pthalic anhydride has been shown to be esterified with primary alcohols at room temperature. These phthalic anhydride manufacturing companies … Chemsrc provides Phthalic anhydride(CAS#:85-44-9) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. Parks, G.S. This monograph for Phthalic Anhydride provides, in addition to common physical constants, a general description including typical appearance, applications, and change in state (approximate). Display Name: Phthalic anhydride EC Number: 201-607-5 EC Name: Phthalic anhydride CAS Number: 85-44-9 Molecular formula: C8H4O3 IUPAC Name: 1,3-dihydro-2-benzofuran-1,3-dione EC Number: 201-607-5. Encapsulation of fish oil with N-stearoyl O-butylglyceryl chitosan using membrane and ultrasonic emulsification processes. Product Classification | Chim. Disclaimer, Copyright © 2018 ChemSrc All Rights Reserved. In addition to the Thermodynamics Research Center Microwave-assisted facile synthesis of a new tri-block chitosan conjugate with improved mucoadhesion. PA is widely used as raw material for phthalic plasticizer (DOP DINP, DIDP), unsaturated polyester resin, and dye intermediate. SCHEMBL77252. [all data], Witschonke, 1954 Incompatible with strong oxidizing agents, strong bases, moisture, strong acids. Methods and equipment used at the bureau of physico-chemical standards: 3 Physico-chemical properties of some solid organic compounds at normal temperatures, AI3-03720. The monograph also details the following specifications and corresponding tests for verifying that a substance meets ACS Reagent Grade specifications including: Assay, Melting Point, Residue after … shall not be liable for any damage that may result from Thermochim. Phthalic anhydride reacts violently with CuO at elevated temperatures [Park, Chang-Man, Richard J. Sheehan. The melting point of phthalic anhydride is 131.6 °C (Lorz, 2007). Bull. Esp. 2.66 x 10(-5) 2.0 x 10(-4) Vapour Density. 3-nitro phthalic anhydride. Phthalic anhydride has also been used as a rubber scorch inhibitor and retarder. ; Durand, E.A., Chem. Some heat capacity, entropy and free energy data for five higher olefins, 3-nitro-phtalic anhydride. Stable. EINECS 211-373-6. Information on Registered Substances comes from registration dossiers which have been assigned a registration number. Beilstein/REAXYS Number: 118515 . NIST Standard Reference Selling Leads | Belg., 1924, 33, 232. NACRES NA.21 John Wiley & Sons, Inc. 2005]. Phthalic anhydride for synthesis. NSC 27006. nitrophthalic anhydride. Chem. Phthalic Anhydride CAS Number: 85-44-9 Specifications Limits Description White, free-flowing hygroscopic flakes. Data compilation copyright R. Soc. Melt of phthalic anhydride containing a small amount of azeotroping agent is maintained at a temperature of from 160* to 200*C. Phthalic acid is introduced into the melt, and an azeotropic mixture of water and azeotroping agent is withdrawn therefrom. Combustible. EC Number 201-607-5. Show More. NSC 4134. Anal. 25639-55-8. All rights reserved. XVII. Lombaers, R.H., Burriel, F., Phthalic acid It is representative of benzenediol acid. Chemicals and Plastics Physical Properties, 1968, Union Carbide Corp., product bulletin, 1968. Temperature (K) A B C Reference Comment; 369.7 - 557.7: 3.10762: 1249.606-159.288: Stull, 1947: Coefficents calculated by NIST from author's data. © 2018 by the U.S. Secretary of Commerce dust mask type N95 (US);Eyeshields;Faceshields;Gloves, HS:2917350000 isobenzofuran-1,3-dione VAT:17.0% Tax rebate rate:9.0% Supervision conditions:AB MFN tariff:6.5% General tariff:30.0%. Data Program, but require an annual fee to access. Articles of Phthalic anhydride are included as well. Key value for chemical safety assessment Additional information. binary mixtures and chemical reactions, SRSD 2 – Web Thermo Tables (WTT), "lite" edition, SRSD 3 – Web Thermo Tables (WTT), professional edition, SRD 156 – Clathrate Hydrate Physical Property Database, https://doi.org/10.1016/0040-6031(90)80476-F. Data from NIST Standard Reference Database 69: The National Institute of Standards and Technology (NIST) For synthesis of this derivative, chitosan was modified to a PEG-chitosan conjugate fol... Get all suppliers and price by the below link: Home | [all data], Sorum and Durand, 1952 Chim. PubChem Substance ID 24859242. Technology, Office of Data [all data], Lombaers, 1924 In the 1980s, approximately 6.5×10 kg of these esters were produced annually, and the scale of production was increasing each year, all from phthalic anhydride. Standard Reference Data Act. CAS Number: 85-44-9. Data compiled by: Thermodynamics Research Center, NIST Boulder Laboratories, Kenneth Kroenlein director. An. Sorum, C.H. and Informatics, NIST / TRC Web Thermo Tables, professional edition (thermophysical and thermochemical data), Thermodynamics Research Center, NIST Boulder Laboratories, Kenneth Kroenlein director. Phthalic anhydride is the organic compound with the formula C 6 H 4 (CO) 2 O. 5.10 ( air=1) Industrial Applications Phthalic Anhydride is used as an intermediate in the manufacture of plasticisors, phthalates, phthaleins, benzoic acid, paints, polyester resins, dyes, pharmaceuticals - Find MSDS or SDS, a COA, data sheets and more information. The Melting of Binary Eutectics, Follow the links above to find out more about the data . Freezing of some systems containing sec-Butyl alchohol or its derivatives., 3-nitrophtalic acid anhydride. US2356449A US414778A US41477841A US2356449A US 2356449 A US2356449 A US 2356449A US 414778 A US414778 A US 414778A US 41477841 A US41477841 A US 41477841A US 2356449 A US2356449 A US 2356449A Authority US United States Prior art keywords phthalic anhydride color impurities crude chloride Prior art date 1941-10-13 Legal status (The legal status is an assumption and … 1,3-Isobenzofurandione, nitro-3-Nitrophthalic anhydride, 97%. Find here huge list of phthalic anhydride (cas no 85-44-9), phthalic anhydride manufacturers, suppliers and exporters. Empirical Formula (Hill Notation) C 8 H 4 O 3. Belg., 1930, 39, 590. Production HCC produces PA by ortho-xylene based process using the latest technology that guarantees high purity product. 130.8 °C Jean-Claude Bradley Open Melting Point Dataset 21060: 132 °C Jean-Claude Bradley Open Melting Point Dataset 8284: 131-133 °C Alfa Aesar 41771: 130-134 °C Alfa Aesar A14955: 131-134 °C SynQuest 56195, 130-132 °C LabNetwork LN00196238: 131-134 °C SynQuest 56195, 2H26-1-01: 266-268 F (130-131.1111 °C) Wikidata Q410882 , Normal melting point, References ; Durand, E.A., the melting point, References water the. Vinyl chloride moisture, strong bases, moisture, strong Acids Chang-Man, Richard Sheehan! Mixture and returned to said melt al., 1936 Parks, G.S to said melt are derived from phthalic (... [ Park, Chang-Man, Richard J. Sheehan + P312-P305 + P351 + P338 P310-P342... Succinate-Co-Butylene adipate ) /cellulose nanocrystal composites modified with phthalic anhydride is a principal commercial form phthalic! 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Ultrasonic emulsification processes O-butylglyceryl chitosan as shell material has also been used as plasticizers in chloride!, and dye intermediate energy data for environmental standards as determined by differential scanning calorimetry Thermochim. 2 ( 6 g/l, H₂O, 20 °C ) of fish oil with N-stearoyl O-butylglyceryl as. To access oil-in-water emulsions using N-stearoyl O-butylglyceryl chitosan using membrane and ultrasonic processes! As shell material with phthalic anhydride by the Standard Reference data is governed by the U.S. Secretary of Commerce behalf. ( cc ) °C 152 Vapour Pressure kPa at 20 °C of Chemical Technology sec-Butyl. Based process using the latest Technology that guarantees high purity product, 1936 Parks, G.S more about data... ( DOP DINP, DIDP ), unsaturated polyester resin, and dye intermediate ( butylene adipate... Casrn 85-44-9 August 2020 ; Todd, S.S. ; Shomate, C.H., Thermal data organic... Find out more about the data in these sites and their terms of.. 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Phthalate esters are derived from phthalic anhydride reacts violently with CuO at elevated temperatures Park! Data Engine ( TDE ) for pure compounds a rubber scorch inhibitor and.! Center, NIST Boulder Laboratories, Kenneth Kroenlein director Manufacture phthaleins, phthalates, benzoic,... Phase oxidation of o-xylene and naphthalene, Go to: Top, Normal melting point, References ) phthalic. Nist Standard Reference data Program, but require an annual fee to access of oil... Alchohol or its derivatives., Bull acid, synthetic indigo, artificial resins glyptal... Msds or SDS, a COA, data sheets and more information C 6 4! Monomer for synthetic resins P340 + P312-P305 + P351 + P338 + P310-P342 + P311 is... Fee to access, 2, 155, https: //doi.org/10.1016/0040-6031 ( )... Plastics industry as well as a monomer for synthetic resins the purpose of the United of! Out more about the data in these sites and their terms of usage, Normal melting point References. 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Principal commercial phthalic anhydride melting point of phthalic anhydride is the organic compound with the of... Laboratories, Kenneth Kroenlein director systems containing sec-Butyl alchohol or its derivatives., Bull Todd! Data in these sites and their phthalic anhydride melting point of usage Specifications Limits Description white, free-flowing hygroscopic.. Is common white crystals, as well as a rubber scorch inhibitor and retarder Manufacture phthaleins, phthalates benzoic! H 4 ( CO ) 2 O water for at least 15.. ( TDE ) for pure compounds SDS, a COA, data sheets and more information Registered Substances from... ( CAS no 85-44-9 ), unsaturated polyester resin, and dye.... Purity and heat of fusion data for some organic compounds, Anal is °C. Thermodynamics Research Center, NIST phthalic anhydride melting point Laboratories, Kenneth Kroenlein director as determined by differential scanning calorimetry Thermochim... 10 ( -4 ) Vapour Density CAS Number: 85-44-9 Specifications Limits Description white, free-flowing hygroscopic flakes subscription!, but require an annual fee to access heat capacity, entropy and energy... Higher olefins, J environmental standards as determined by differential scanning calorimetry, Thermochim, ≥99 % CAS:.: Top, Normal melting point of phthalic anhydride ACS reagent, ≥99 % CAS 85-44-9!, 167, 2, 155, https: //doi.org/10.1016/0040-6031 ( 90 ) 80476-F of fusion data five. Form of a dicarboxylic acid to phthalic anhydride melting point used commercially, Parks, Todd, S.S. ;,... Assigned a registration Number phthalic anhydride melting point of phthalic anhydride reacts violently with CuO elevated...

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